TY - JOUR
T1 - N,N′-dichloro-p-nitrobenzenesulfonamide (dichloramine-N) as a new oxidimetric reagent
T2 - Synthesis and analytical application
AU - Made Gowda, Netkal M.
AU - Ramanujam, V. M.Sadagopa
AU - Trieff, Norman M.
AU - Stanton, G. John
AU - Mahadevappa, Dandinasivara S.
N1 - Funding Information:
This study was supportedb y the James W. McLaughlin Fellowship Fund (Grant to Drs. NMT, GJS, and NMMG) and the Robert A. Welch Foundation( Grant H-416t o Dr. NMT). The authorsa lso thank Dr. D. J. Leggett, Departmento f Chemistry, University of Houston, Texas for the ‘H and 13CN MR spectra.
PY - 1981/3
Y1 - 1981/3
N2 - A new oxidimetric reagent, dichloramine-N (N,N′-dichloro-p-nitrobenzenesulfonamide; DCN) has been synthesized and its structure elucidated from the spectral data and elemental analyses. The ultraviolet, infrared, nuclear magnetic resonance, and mass spectral data have been presented. Analytical applications of DCN as a potential redox titrant in the determination of diverse reductants such as ascorbic acid, methionine, sulfite, arsenite, glutathione, and indigocarmine have been described.
AB - A new oxidimetric reagent, dichloramine-N (N,N′-dichloro-p-nitrobenzenesulfonamide; DCN) has been synthesized and its structure elucidated from the spectral data and elemental analyses. The ultraviolet, infrared, nuclear magnetic resonance, and mass spectral data have been presented. Analytical applications of DCN as a potential redox titrant in the determination of diverse reductants such as ascorbic acid, methionine, sulfite, arsenite, glutathione, and indigocarmine have been described.
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U2 - 10.1016/0026-265X(81)90015-1
DO - 10.1016/0026-265X(81)90015-1
M3 - Article
AN - SCOPUS:0347872268
SN - 0026-265X
VL - 26
SP - 95
EP - 104
JO - Microchemical Journal
JF - Microchemical Journal
IS - 1
ER -